Defining Plate Height overhead(24-5)
Kinetics / The VanDeemter Equn / Column Efficiency overheads
H = B/u + Csu + Cmu
GAS CHROMATOGRAPHY
- Gas-Liquid- Gas-Solid
- Capillary
- Carrier gases
- inert Argon, Helium, Nitrogen,CO2, H2.
- normal flow rates 10-50psi inlet pressure
flow = 25-150mL/min with packed
1-25mL/min cap
- Sample injection
introduce sample as a plug
typical injector overhead
- Columns and Temperatures
- most are cap.
- glass, fused silica, teflon 2m to 150m long with 0.1-0.5mm id
- some packed 1m max with 2-4mm id overhead
-
Fixed Temperature, or Ramped T
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This document was last modified on Sunday, January 31 1999.